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[platne_od] => 31.10.2023 17:11:00
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Technická 5
166 28 Prague 6 – Dejvice
IČO: 60461373 / VAT: CZ60461373
Czech Post certified digital mail code: sp4j9ch
Copyright: UCT Prague 2015
Information provided by the Department of International Relations and the Department of R&D. Technical support by the Computing Centre.
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[obsah] => Department of Solid State Chemistry is focused on materials, methods (X-ray diffraction analysis), and industry applications. A wide choice of Bc., MSc., and Ph.D. programs comprises chemistry and technology of inorganic materials, X-ray diffraction analysis for the pharmaceutical industry, and heavy metal migration in the environment.
The research work of the department deals with two basic topics:
- Application of X-ray diffraction methods in pharmaceutical industry, research, production, and quality check
- Applied mineralogy
History of Department
The staff of the Department follows the tradition of the former Department of Mineralogy. Professor F. X. M. Zippe has established mineralogical collections in 1835, which were later enriched and perfected by Professor A. Ondřej (1887-1956). The mineralogical collections are the well-known treasure of the institute. The X-ray diffraction methods were introduced to our department in 1945 and have remained the prime analytical method of our department.
Cooperation
The Department has an official
cooperation with the company Teva Czech Industries s. r. o. since 1991.
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The research work of the department deals with three topics:
- Application of X-ray diffraction methods in pharmaceutical industry, research, production and quality check
- Applied mineralogy
- Migration of heavy metals in the environment
History of department
Staff of the Department follows the tradition of the former Department of Mineralogy. Professor F. X. M. Zippe has established mineralogical collections in 1835, which were later enriched and perfected by Professor A. Ondřej (1887-1956). The mineralogical collections are the well-known treasure of the institute. The X-ray diffraction methods were introduced to our department in 1945 and have remained the prime analytical method of our department.
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[obsah] => Research at the Institute deals with two thematic areas
- Application of X-ray structural and phase analysis in pharmaceutical research, development, production and control.
- Monitoring of polymorphism of active pharmaceutical substances by X-ray diffraction analysis methods and development of this methodology
- Zeolites
- Transport of heavy metals in the environment
- Double layered hydroxides
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History of the collections
Mineralogical collections at the Prague Institute of Chemical Technology belong to the oldest and best organized university collections. They are internationally registered in a list of world-known collections in Europe.
The first mineralogical collections was created by professor F. X. M. Zippe for pedagogic purposes of the Technical College in Prague in the year 1835. The basis of this collection has enlarged professor Jan Krejci, whose detailed catalogue of minerals issued in the year 1899 has been preserved till the present days. After the first world war the head of the Mineralogy Department was professor Augustin Ondrej. He made his life goal to finish and shape the mineralogical collections in such form which would well serve also to the next generation as a basis of science and pedagogic work. Purchases, donations, collecting expeditions and numerous exchanges have increased the collection from 2 102 to 23 861 inventory numbers. This was also the last entry of professor Ondrej, who passed away on 22 nd July 1956. His successor professor Jan Kaspar visited his life-time perhaps all continents of the world, studying minerals and their deposites. He collected minerals in all countries he visited.
Organization of collections
In the present form the mineralogical collections cover several units. In the first place is the systematic collection which is located in the main large collection hall. In an adjacent smaller room there is the collection of decorative and gem stones. Supplementary collections are located in the corridor in front of the main hall. They include crystalographical, terminological and petrographical collections and further the collections of industrial and technical raw materials. In the so called small collection hall geaochemical and genetic collectioons of minerals are installed. Here are also exhibited collections of meteorites and tektites.
Visiting of the collections
You can visit our mineralogical collections as follows:
Monday - Thursday: 9:00 - 16:00
Friday: 9:00 - 14:00
You must arrange the visit by e-mail or by phone with the secretary (+420-220443798) or with head of department (+420-220444086).
Photos:
 |
 |
| Decoration and precious stones coll. |
Glass models of diamonds |
 |
 |
| Model of gold and platinum nuggets |
Models of crystal types |
 |
 |
| Petrographic collection |
Corridor in front of main hall |
 |
 |
| Meteorite collection |
Main collection hall |
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DATA
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[seo_title] => List of selected papers
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[obsah] => Nievergelt, P. P.; Babor, M.; Cejka, J.; Spingler, B. A high throughput screening method for the nano-crystallization of salts of organic cations. Chemical Science 2018 9(15), 3716-3722.
Dolensky, B.; Kessler, J.; Jakubek, M.; Havlik, M.; Cejka, J.; Novotna, J.; Kral, V., Synthesis and characterisation of a new naphthalene tris-Troger's base derivative-a chiral molecular clip. Tetrahedron Letters 2013, 54, 308-311.
Skorepova, E.; Cejka, J.; Husak, M.; Eigner, V.; Rohlicek, J.; Sturc, A.; Kratochvil, B., Trospium Chloride: Unusual Example of Polymorphism Based on Structure Disorder. Crystal Growth & Design 2013, 13, 5193-5203.
Urbanova, M.; Sturcova, A.; Brus, J.; Benes, H.; Skorepova, E.; Kratochvil, B.; Cejka, J.; Sedenkova, I.; Kobera, L.; Policianova, O.; Sturc, A., Characterizing crystal disorder of trospium chloride: A comprehensive,13C CP/MAS NMR, DSC, FTIR, and XRPD study. Journal of Pharmaceutical Sciences 2013, 102, 1235-1248.
Skorepova, E.; Husak, M.; Cejka, J.; Zamostny, P.; Kratochvil, B., Increasing dissolution of trospium chloride by co-crystallization with urea. Journal of Crystal Growth 2014, 399, 19-26.
Pazout R., Maixner., Dusek M., Kratochvil B.: A new polymorph of succinylcholinium diiodide: comparison of succinylcholinium structures. Acta Crystallogr C 67 (2011), O391-O393.
Kratochvil B., Koupilova I.: Pharmaceutical amorphous hydrates. Chem Listy 105 (2011), 3-7.
Kratochvil B.: Solid forms of pharmaceutical molecules. In: Glassy, amorphous and disordered materials: thermal physics, analysis, structure and properties. (Jaroslav Sestak, Jiri J. Mares and Pavel Hubik Eds.). Springer Verlag.
Okavoca L., Vetchy D., Franc A., Rabiskova M., Kratochvil B.: Increasing bioavailability of poorly water-soluble drugs by their modification. Chem Listy 104 (2010), 21-26.
Kratochvil B., Husak M., Brynda J. et al.: What Can the Current X-Ray Structure Analysis Offer? Chem listy 102 (2008), 889-901.
Hajkova M., Kratochvil B., Radl S.: Atorvastatin - the world´s best selling drug. Chem Listy 102 (2008), 3-14.
Kratochvil B.: Crystallization of Pharmaceutical Substances. Chem listy 101 (2007), 3-12.
Jegorov A., Petrickova H., Kratochvil B., Cisarova I.: An unusual cis-dichloro[17-(cyclobutylmethyl)3-methoxymorphinan-14-ol- N,O] palladium(II) complex. Collect Czech Chem C 71 (2006), 434-442.
Chudik M., Jegorov A., Petrickova H., Kratochvil B., Cisarova I.: Crystal structure of 3-benzoylmorphin-6-one-17-carboxamide ethanol solvate (1 : 0.333), C24H20N2O5 center dot 0.333C(2)H(5)OH. Z Krist-New Cryst St 220 (2005), 348-350.
Kratochvil B.: Crystal lattice - What with it? Chem Listy 99 (2005), 258-259.
Kratochvil B., Belohlav Z.: Involvement of Institute of Chemical Technology Prague in the research and manufacturing of pharmaceuticals. Chem Listy 98 (2004), 1140-1142.
Kratochvil B., Husak M., Jegorov A.: Polymorphism and solvatomorphism of solid substances in pharmacy.Chem listy 96 (2002), 330-335.
Kamenicek J., Valach F., Kratochvil B., Zak Z.: Syntheses and structure of Ni(III) complexes with 1-toluene-3,4-dithiole. Bond-valence approach to the oxidation state of the central atom. Pol J Chem 76(2002), 483-490.
Krarochvil B., Husak M., Jegorov A.: Conformational flexibility of cyclosporins. Chem Listy 95 (2001), 9-17.
Pohl R., Sykora J., Malon P., Bohm S., Kratochvil B., Kuthan J.: Sterically crowded heterocycles. XIII. An insight into the absolute stereochemistry of atropisomeric (Z)-3-(imidazo[1,2-a]pyridin-3-yl)prop-2-en-1-ones.Collect Czech Chem C 65 (2000), 1643-1652.
Kratochvil B., Jegorov A., Pakhomova S., Husak M., Bulej P., Cvak L., Sedmera P., Havlicek V.: Crystal structures of cyclosporin derivatives: O-acetyl-(4R)-4-(E-2-butyl)-4,N-dimethyl-L-threonyl-cyclosporin A and O-acetyl-(4R)-4-[E-2-(4-bromobutyl)]-4,N-dimethyl-L-threonyl-cyclosporin A. Collect Czech Chem C 64(1999), 89-98.
Pakhomova S., Kratochvil B., Lellek V., Stibor I.: Methyl 3 ',6 '-bis(chloromethyl)-2,2 '-dimethoxy-1,1 '-binaphthalene-3-carboxylate. Acta Crystallogr 53 (1997), 1871-1873.
Cvak L., Jegorov A., Pakhomova S., Kratochvil B., Sedmera P., Havlicek V., Minar J.: 8 alpha-hydroxy-alpha-ergokryptine, an ergot alkaloid. Phytochemistry 44 (1997), 365-369.
Cvak L, Minar J, Pakhomova S, Ondracek J, Kratochvil B, Sedmera P, Havlicek V, Jegorov A.: Ergoladinine, an ergot alkaloid. Phytochemistry 42 (1996), 231-233.
Husak M., Gabriel R.: Case Study of Polymorphic Transformation. Chem Listy 105 (2011), 381-384.
Husak M., Kratochvil B., Jegorov A. et al.: Simvastatin: Structure Solution of Two New Low-Temperature Phases from Synchrotron Powder Diffraction and ss-NMR. Struct Chem 21 (2010), 511-518.
Husak M., Jegorov A., Brus J. et al.: Metergoline II: Structure Solution from Powder Diffraction Data with Preferred Orientation and from Microcrystal. Struct Chem 19 (2008), 517 - 525.
Husak M., Rohlicek J., Cejka J., Kratochvil B.: Structure determination from powder diffraction data - It is unrealizable dream or daily use? Chem Listy 101 (2007), 697-705.
Jegorov A., Cvak L., Bednar R., Cejka J., Husak M., Kratochvil B., Cisarova I.: Structures of cabergoline anhydrate form II and novel cabergoline solvates. Struct Chem 17 (2006), 131-137.
Husak M., Kratochvil B., Cisarova I. et al.: Crystal structure of (1-ethoxycarbonyl-pentadecyl)-trimethyl ammonium bromide, (C21H44NO2)Br, form I. Z Krist - New Cryst St 219 (2004), 439 - 441.
Bulej P., Kuchar M., Husak M., Kratochvil B., Jegorov A.: Crystal structure of 4-(2 ',4 '-difluorobiphenyl-4-yl)-2-methylbutanoic acid, F2C16H15COOH, deoxoflobufen. Z Krist - New Cryst St 219 (2004), 297-298.
Husak M., Kratochvil B., Cisarova I., Cvak L., Jegorov A., Bohm S.: Crystal forms of semisynthetic ergot alkaloid terguride. Collect Czech Chem C 67 (2002), 479-489.
Husak M., Kratochvil B., Cisarova I., Jegorov A.: Crystal structures of two new cyclosporin clathrates.Collect Czech Chem C 65 (2000), 1950-1958.
Jegorov A., Cvak L., Husek A., Simek P., Heydova A., Ondracek J., Pakhomova S., Husak M., Kratochvil B., Sedmera P., Havlicek V.: Synthesis and crystal structure determination of cyclosporin H. Collect Czech Chem C 65 (2000), 1317-1328.
Jegorov A., Pakhomova S., Husak M., Kratochvil B., Zak Z., Cvak L., Buchta M.: Cyclosporins of symmetry P2(1) - a series of clathrates. J Incl Phenom Macro 37 (2000), 137-153.
Husak M., Kratochvil B., Jegorov A.: Crystal structure of ergometrine ethyl acetate solvate (2 : 1), (C19H23N3O2)(2)(C4H8O2). Z Krist - New Cryst St 213 (1998), 195-196.
Husak M., Kratochvil B., Sedmera P., Havlicek V., Votavova H., Cvak L., Bulej P., Jegorov A.: Molecular structure of cis- and trans-tergurides. Collect Czech Chem C 63 (1998).
Husak M., Kratochvil B., Buchta M., Cvak L., Jegorov A.: Crystal structure of cyclosporin E. Collect Czech Chem C 63 (1998), 115-120.
Rohlíček J., Hušák M.: MCE2005 – a new version of a program for fast interactive visualization of electron and similar densitymaps optimized for small molecules. J Appl Crystallogr 40 (2007), 600-601.
Rohlicek J., Maixner J., Pazout R. et al.: Alaptide from Synchrotron Powder Diffraction Data. Acta Crystallogr E 66 (2010), O821-U2229.
Rohlicek J., Husak M., Kratochvil B. et al.: Methylergometrine Maleate from Synchrotron Powder Diffraction Data. Acta Crystallogr E 65 (2009), O3252-U1981.
Rohlicek J., Husak M., Gavenda A. et al.: Capecitabine from X-Ray Powder Synchrotron Data. Acta Crystallogr E 65 (2009), O1325-U2267.
Dolensky B., Kvicala J., Paleta O., Lang J., Dvorakova H., Cejka J.: Trifluoromethylated (tetrahydropyrrolo) quinazolinones by a new three-component reaction and facile assignment of the regio- and stereoisomers formed by NMR spectroscopy. Magn Reson Chem 48 (2010), 375-385.
Tatar A., Cejka J., Kral V., Dolensky B.: Spiro Troger's Base Derivatives: Another Structural Phoenix? Org Lett 12 (2010), 1872-1875.
Sergeyev S., Stas S., Remacle A., Velde CMLV, Dolensky B., Havlik M., Kral V., Cejka J.: Enantioseparations of non-benzenoid and oligo-Troger's bases by HPLC on Whelk O1 column. Tetrahedron-Asymmetr 20 (2009), 1918-1923.
Valik M., Cejka J., Havlik M., Kral V., Dolensky B.: Calix-Tris-Troger's bases - a new cavitand family.Chem Commun 37 (2007), 3835-3837.
Jegorov A., Cvak L., Bednar R., Cejka J., Husak M., Kratochvil B., Cisarova I.: Structures of cabergoline anhydrate form II and novel cabergoline solvates. Struct Chem 17 (2006), 131-137.
Cejka J., Kratochvil B., Cvak L. et al.: Crystal structure of 2-bromo-1 '-alpha beta-dehydro-ergokryptam acetone sesquisolvate, C32H38BrN5O4 center dot 1.5 (CH3)(2)CO. Z Krist - New Cryst St 220 (2005), 345-347.
Klepetarova B., Cejka J., Kratochvil B., Pakhomova S., Cisakova I., Cvak L., Jegorov A.: Interesting solvent area in crystal structures of two natural ergot alkaloids. Collect Czech Chem C 70 (2005), 41-50.
Cejka J., Kratochvil B., Cisarova I. et al.: Simvastatin. Acta Crystallogr C 59 (2003), O428-O430.
Cejka J., Kratochvil B., Bohm S. et al.: Structural Study of Dopamine Agonist Lisuride. Collect Czech Chem C 68 (2003), 2150-2158.
Petrickova H., Cejka J., Husak M., Kratochvil B., Cisarova I., Jegorov A., Cvak L.: Structure types of dihydroergotoxine mesylates. Collect Czech Chem C 67 (2002), 490-501.
Curinova P., Pojarova M., Budka J., Lang K., Stibor I., Lhotak P.: Binding of neutral molecules by p-nitrophenylureido substituted calix[4]arenes. Tetrahedron 66 (2010), 8047-8050.
Holakovsky R., Pojarova M., Dusek M., Cejka J., Cisarova I.: (R)-2,2 '-Bis[N '-(3,5-dichlorophenyl)ureido]-1,1 '-binaphthalene chloroform disolvate. Acta Crystalogr E - Structure Reports Online 67 (2011), O384-U806.
Kundrat O., Dvorakova H. Cisarova I., Pojarova M., Lhotak P.: Unusual Intramolecular Bridging Reaction in Thiacalix[4]arene Series. Org Lett 11 (2009), 4188-4191.
Machar A., Kozmik V., Pojarova M. et al.: Preparation and Rearrangement Study of Novel Thiophenium- and Selenophenium-Ylides. Collect Czech Chem C 74 (2009), 785-798.
Kundrat O., Cisarova I., Bohm S., Pojarova M., Lhotak P.: Uncommon Regioselectivity in Thiacalix[4]arene Formylation. J Org Chem 74 (2009), 4592-4596.
Kroupa J., Stibor I.,Pojarova M. Tkadlecova M., Lhotak P.: Anion receptors based on ureido-substituted thiacalix[4]arenes and calix[4]arenes. Tetrahedron 64 (2008), 10075-10079.
Lhotak P., Bila A., Budka J., Pojarova M., Stibora I.: Simple synthesis of calix[4]arenes in a 1,2-alternate conformation. Chem Commun 14 (2008), 1662-1664.
Lang K., Proskova P., Kroupa J., Moravek J., Stibor I., Pojarova M., Lhotak P.: The synthesis and complexation of novel azosubstituted calix[4]arenes and thiacalix[4]arenes. Dyes Pigments 77 (2008), 646-652.
Pojarova M., Kaufmann D., Gaspar R., Nishino T., Reszka P., Bednarski P.J., von Angerer E.: [(2-Phenylindol-3-yl)methylene]propanedinitriles inhibit the growth of breast cancer cells by cell cycle arrest in G(2)/M phase and apoptosis. Bioorgan Med Chem 15 (2007), 7368-7379.
Pojarova M., Ananchenko G.S., Udachin K.A. et al.: Alpha-C=O Provides Access to the Cavity in Acyl Calix[4]arenes Nanocapsules. New J Chem 31 (2007), 871-878.
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